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Mesoporous silica of SBA-15 kind was modified for the primary time with 3-(trihydroxysiyl)-1-propanesulfonic acid (TPS) by post-synthesis modification involving microwave or conventional heating to be able to generate the Brønsted acidic centers on the material surface. The samples structure and composition had been examined by low temperature N2 adsorption/desorption, XRD, HRTEM, elemental and thermal analyses. The floor properties had been evaluated by esterification of acetic acid with n-hexanol used as the take a look at reaction. A a lot increased efficiency of TPS species incorporation was reached with the applying of microwave radiation for 1 h than standard modification for 24 h. It was found that the structure of mesoporous assist was preserved after modification using both methods applied on this research. Materials obtained with the use of microwave radiation showed a superior catalytic activity and high stability. Engaged on a manuscript? The construction of those solids is characterized by comparatively giant floor area, e.g. A thousand m2 g−1, and the presence of hexagonal channels regular in dimension.